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3 4-Dichlorophenylhydrazine hydrochloride (CAS # 19763-90-7)

Chemical Property:

Molecular Formula C6H7Cl3N2
Molar Mass 213.49 Nws
Melting Point 230 ° C (txog) (lit.)
Boling Point 288.3 ° C ntawm 760 mmHg
Flash Point 128.2°C dej
Vapor Siab 0.00236mmHg ntawm 25 ° C
Qhov tshwm sim Dawb hmoov
BRN 3703934 ib
Kev cia khoom nyob rau hauv inert gas (nitrogen los yog Argon) ntawm 2-8 ° C
MDL PAB 00012937

Product Detail

Khoom cim npe

Risk thiab Safety

Risk Codes R20/21/22 - Ua phem los ntawm kev nqus pa, tiv thaiv daim tawv nqaij thiab yog tias nqos.
R36/37/38 - Kab mob rau qhov muag, ua pa thiab tawv nqaij.
Kev nyab xeeb piav qhia S26 - Thaum sib cuag nrog lub qhov muag, yaug tam sim ntawd nrog dej txaus thiab nrhiav kev kho mob.
S37/39 - Hnav cov hnab looj tes tsim nyog thiab tiv thaiv qhov muag / ntsej muag
S36/37/39 - Hnav cov khaub ncaws tiv thaiv tsim nyog, hnab looj tes thiab tiv thaiv qhov muag / ntsej muag.
S22 - Tsis txhob nqus plua plav.
S24/25 - Tsis txhob sib cuag nrog daim tawv nqaij thiab qhov muag.
UN IDs 2811 ib
WGK Germany 3
HS Code 29 280 000 ib
Kev Ceeb Toom Ua phem/Irritant
Hazard Class IRRITANT

 

 

3 4-Dichlorophenylhydrazine hydrochloride (CAS # 19763-90-7) Cov ntaub ntawv

daim ntawv thov 3, 4-dichlorophenylhydrazine hydrochloride yog ib qho tshuaj nruab nrab uas siv tau los npaj biphenylpyridine.
txoj kev npaj 3,4-dichloroaniline (38.88g, 0.2399mol) yog yaj hauv dichloroethane (30ml), tom qab ntawd 12mol / L concentrated hydrochloric acid (70ml, 0.84mol) ntxiv, sodium nitrite (18.06g, 0.261mol) ntxiv, cov tshuaj tiv thaiv yog nplawm ntawm 5 ℃ rau 30min, thiab cov kua ntshiab lim tau lim tawm, poob mus rau 140ml ntawm sodium sulfite tov uas muaj (90.71g, 0.7197mol), teb ntawm 80 ℃ li 3 teev, react los tsim 3,4-dichlorophenylhydrazine, ntxiv txog (60ml, 0.72mol) concentrated hydrochloric acid rau 1 teev, do. hmo ntuj ntawm chav tsev kub, lim kom tau 3,4-dichlorophenylhydrazine hydrochloride dawb khoom 46.1 g, yoj: 90%.

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  • Sau koj cov lus ntawm no thiab xa tuaj rau peb