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4-Methoxyphenylhydrazine hydrochloride (CAS # 19501-58-7)

Chemical Property:

Molecular Formula C7H11ClN2O
Molar Mass 174.63 ib
Melting Point 160-162 ° C (hnub) (lit.)
Boling Point 263.5 ° C ntawm 760 mmHg
Flash Point 113.2°C dej
Dej Solubility soluble
Vapor Siab 0.0103mmHg ntawm 25 ° C
Qhov tshwm sim Grey daj liab liab khoom
Xim Me ntsis liab rau grey rau ntshav
BRN 3 566583
Kev cia khoom Cia txias
MDL PAB 00012945
Physical thiab Chemical Properties Melting point 160-162 ° C (dec.)
dej-soluble soluble
Siv Siv rau dyes thiab kws tshuaj intermediates.

Product Detail

Khoom cim npe

Risk thiab Safety

Risk Codes R20/21/22 - Ua phem los ntawm kev nqus pa, tiv thaiv daim tawv nqaij thiab yog tias nqos.
R36/37/38 - Kab mob rau qhov muag, ua pa thiab tawv nqaij.
Kev nyab xeeb piav qhia S36/37 - Hnav cov khaub ncaws tiv thaiv thiab hnab looj tes tsim nyog.
S36 - Hnav khaub ncaws tiv thaiv zoo.
S26 - Thaum sib cuag nrog lub qhov muag, yaug tam sim ntawd nrog dej txaus thiab nrhiav kev kho mob.
UN IDs 2811 ib
WGK Germany 3
HS Code 29280090 ib
Kev Ceeb Toom Irritant/Homful
Hazard Class TSIS TXAUS SIAB, Cia txias
Packing Group III

 

 

4-Methoxyphenylhydrazine hydrochloride (CAS # 19501-58-7) Cov ntaub ntawv

Siv 4-methoxyphenylhydrazine hydrochloride yog ib qho nruab nrab, feem ntau yog siv los tsim cov phenylhydrazine tebchaw, thiab tseem tuaj yeem siv los tsim lwm yam khoom siv tshuaj, xws li 4-nitroindole thiab apixaban.
Siv rau dyes thiab kws tshuaj intermediates
Kev npaj 4-methoxyphenylhydrazine hydrochloride tuaj yeem npaj los ntawm aniline los ntawm cov tshuaj tiv thaiv diazotization.
Noj aniline, hydrochloric acid thiab sodium nitrite, molar ratio ntawm lawv yog 1: 3.2: 1.0, ua ntej ntxiv hydrochloric acid, ces ntxiv ammonium nitrite ntawm 5 ℃, thiab react ntawm 0 ~ 20 ℃ rau 40 feeb los tsim chlorinated diazbenzene; Raws li cov molar ratio ntawm aniline mus rau 1: 3.5: 2.5, ammonium sulfite thiab hydrochloric acid yog ntxiv, thiab txo, hydrolysis thiab acidification yog nqa tawm nyob rau hauv lub txo hwj chim, lub sij hawm txo yog 60 ~ 70 feeb, thiab cov hydrolysis thiab acidification. lub sijhawm yog 50 feeb. Ua ntej, ammonium sulfite reacts nrog ntau tshaj hydrochloric acid los tsim ammonium bisulfite, ammonium bisulfite, ammonium sulfite reacts nrog chlorinated dizobenzene rau tsim phenylhydrazine disulfonate, thiab tom qab ntawd reacts nrog hydrochloric acid rau hydrolysis thiab acid tsom xam cov tshuaj tiv thaiv, thiab tom qab spin-drying, 4- methoxyphenylhydrazine hydrochloride yog npaj.

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